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Formation and Structure of Polyacrylamide–Silica Nanocomposites by Sol–Gel Process

Cited 58 time in Web of Science Cited 59 time in Scopus
Authors
Jang, Jyongsik; Park, Hwanseok
Issue Date
2002
Publisher
Wiley-Blackwell
Citation
Journal of Applied Polymer Science, 2002, 83, 1817–1823
Keywords
polyacrylamide–silica nanocompositesatomic force microscopyhydrogen bondingsilica gelnanocomposite coating
Abstract
The formation of nanocomposites by the sol–gel reaction of tetraethoxysilane
(TEOS) in polyacrylamide (PAAm) is studied. The nanocomposites are prepared in
aqueous solution. Fourier transform IR spectroscopy shows that substantial hydrogen
bonding occurs in the nanocomposites. The fracture surfaces of the nanocomposites are
observed by atomic force microscopy (AFM) as a function of the TEOS content. The
AFM images reveal that the PAAm–silica nanocomposite exhibits particle–matrix
morphology. It is also found that aggregate formation is more dominant than the
particle growth with the TEOS contents. The solution of composite precursor is also
applied to spin coating. Furthermore, during the calcination there is an observable
change in the silica networks, and then a microinterconnected structure is generated.
ISSN
0021-8995
Language
English
URI
http://hdl.handle.net/10371/61941
DOI
https://doi.org/10.1002/app.10116
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College of Engineering/Engineering Practice School (공과대학/대학원)Dept. of Chemical and Biological Engineering (화학생물공학부)Journal Papers (저널논문_화학생물공학부)
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