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Effects of Alloying elements and Rolling Conditions on Stretch Formability of Mg Alloys : 마그네슘 합금 판재 성형성에 미치는 압연 공정 및 첨가 합금의 영향

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dc.contributor.advisor신광선-
dc.contributor.author박중원-
dc.date.accessioned2017-07-13T05:55:54Z-
dc.date.available2017-07-13T05:55:54Z-
dc.date.issued2017-02-
dc.identifier.other000000142657-
dc.identifier.urihttps://hdl.handle.net/10371/118132-
dc.description학위논문 (박사)-- 서울대학교 대학원 : 재료공학부, 2017. 2. 신광선.-
dc.description.abstractThe development of formable Mg sheets is essential to meet the needs of the automotive industry for lightweight material. However, it is difficult to archive high formability due to their crystal structure. Basal slip mode and {10-12} tensile twinning are main deformation modes during deformation at room temperature. An activation of these 2 deformation modes is intricately connected with microstructures, textures, and alloying elements. Various alloys have been developed by using various rolling conditions in order to investigate effects of texture and grain size.
Microstructures and textures of by Mg-Al-Zn, Mg-Zn and Mg-Sn-Al alloys were examined, and then change of IE values through microstructures and textures were investigated. Basal pole intensity significantly decreased in Mg-Al-Zn and Mg-Sn-Al alloys, but there was the slight change in Mg-Zn alloys. In Addition, tensile tests were also performed to investigate the relationship with IE value and corresponding parameters from tensile test such as uniform elongation, the work hardening exponent (n) and the Lankford value (r-value).
To identify effects of grain size and texture on stretch formability more detailed, AZ31 alloys have been developed using various rolling conditions. Increasing rolling temperature enhances the formability of AZ31 alloys because of a weakening basal texture. Increasing annealing temperature and time increase grain size and larger grain size promotes the activation of {10-12} tensile twins. There are two roles of the tensile twinning in deformation. One is to contribute to the deformation through twin strain and another is to support to strain compatibility in grain boundaries. The tensile twins also play a critical role in Erichsen test (bi-axial tension condition).On the other hands, tensile twinning occurring in coarse grain size can decrease the IE value by acting as an origin of cracks because twin growth is so fast that the twin boundary acts as the obstacle interrupting the movement of basal dislocation.
Not only do grain size and texture affect to form {101 ̅2} tensile twins at room temperature, but alloy elements determine twinning, 5 Mg-Zn alloys were fabricated and their grain size varied under different annealing conditions. The large-grain Ca-containing alloy showed the highest amount of {101 ̅2} tensile twin. Tensile twinning is attributed to weak basal texture and large grain size as assessed from measurements of microstructures and VPSC calculations. The results of EBSD analysis and the small Erichsen test reveal that twinning contributes to stretch formability but the interaction between twin and slip causes cracks as grain size increases.
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dc.description.tableofcontentsChapter 1 Introduction 1
1.1 Characterization of Mg and Mg alloys 3
1.2 Twinning in Mg and Mg alloys 9
1.3 Visco-plasticiy self-consistent model 17
1.4 Development of wrought Mg alloys 19
1.5 Research Objectives 21
Bibliography 23
Chapter 2 Experimental procedure 30
2.1 Sample preparation 30
2.1.1 Strip casting and extrusion conditions 30
2.2.2 Rolling and annealing conditions 30
2.2 Characterization of rolled Mg alloys 34
2.2.1 Mechanical properties 34
2.2.2 Microstructure and texture analysis 34
2.2.3 Small Erichsen test 35
2.2.4 Bi-axial tension test 35
Chapter 3 Effects of rolling conditions on stretch formability of Mg alloys 41
3.1 Introductions 41
3.2 Results and discussion 42
3.2.1 Stretch formability vs Rolling conditions 42
3.2.2 Evolution of microstructure and texture 46
3.2.3 Relationship between tensile test and Erichsen test 49
3.3 Conclusions 53
Bibliography 54
Chapter 4 Effects of grain size and texture on mechanical properties of AZ31 56
4.1 Introductions 56
4.2 Results and discussion 60
4.2.1 Results of Erichsen test 60
4.2.2 Microstructure 60
4.2.3 Texture 64
4.2.4 Parameters from tensile tests 67
4.2.5 The role of tensile twin during uniaxial tensile test 73
4.2.6 The role of tensile twin during bi-axial tension test 80
4.2.7 Fracture analysis 83
4.3 Conclusions 90
Bibliography 91
Chapter 5 Effects of alloying elements and rolling condions on stretch formability of Mg-Zn alloys 95
5.1 Introductions 95
5.2 Results and discussion 96
5.2.1 Results of Erichsen test 96
5.2.2 Microstructure 101
5.2.3 Texture 107
5.2.4 Results of tensile test 111
5.2.5 EBSD analysis 116
5.2.6 Relationship between twinning and fracture 118
5.3 Conclusions 122
Bibliography 123
Chapter 6 Effects of alloying elements and rolling conditions on stretch formability of Mg-Al alloys 127
6.1 Introductions 127
6.2 Results and discussion 130
6.2.1 Results of Erichsen test 130
6.2.2 Microstructure and Texture 132
6.2.3 Results of tensile test 139
6.3 Conclusions 150
Bibliography 151
Chapter 7 Summary and conclusions 154
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dc.formatapplication/pdf-
dc.format.extent6665385 bytes-
dc.format.mediumapplication/pdf-
dc.language.isoen-
dc.publisher서울대학교 대학원-
dc.subjectMg alloy-
dc.subjectStretch formability-
dc.subjectTexture-
dc.subjectMicrostructure-
dc.subjectErichsen test-
dc.subject.ddc620-
dc.titleEffects of Alloying elements and Rolling Conditions on Stretch Formability of Mg Alloys-
dc.title.alternative마그네슘 합금 판재 성형성에 미치는 압연 공정 및 첨가 합금의 영향-
dc.typeThesis-
dc.contributor.AlternativeAuthorJoong Won Park-
dc.description.degreeDoctor-
dc.citation.pages157-
dc.contributor.affiliation공과대학 재료공학부-
dc.date.awarded2017-02-
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