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A novel chemoentrapment approach for supportless recycling of a catalyst: Catalytic asymmetric dihydroxylation
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- Authors
- Issue Date
- 2006-06
- Publisher
- Wiley - V C H Verlag GmbbH & Co.
- Citation
- Journal für Praktische Chemie, Vol.348 No.9, pp.1021-1024
- Abstract
- A simple method of recycling a metal catalyst through chemoentrapment in an aqueous layer using ethyl vinyl ether has been developed. Using this new methodology, a highly efficient, filtration-free recycling of osmium for catalytic asymmetric dihydroxylation was accomplished. By means of the formation of a water-soluble OsO42- using EVE, AD reactions of mono- and disubstituted olefins with 1 mol % of OsO4 proceeded for up to 9 cycles without any loss of yields and enantioselectivities.
- ISSN
- 1436-9966
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